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  • Authors: Mai Quan Doan; Nguyen Ha Anh; Nguyen Xuan Quang; Ngo Xuan Dinh; Doan Quang Tri; Tran Quang Huy; Anh-Tuan Le;  Advisor: -;  Co-Author: - (2021)

    An electrochemical approach has been used for green synthesis of gold and silver nanoparticles (e-AuNPs and e-AgNPs) with high levels of purity and scalability. The electrochemically synthesized noble-metal nanoparticles were characterized by ultraviolet–visible (UV–Vis) spectroscopy and scanning electron microscopy (SEM), confirming the formation of spherical e-AuNPs and e-AgNPs with average size of 19 nm and 24 nm, respectively. These green nanoparticles were deposited on aluminum substrates using the drop-drying method for surface-enhanced Raman scattering (SERS)-based detection of Methylene Blue (MB) within the ranges from 10−5 M to 10−8 M and 10−7 M to 10−10 M, respectively. The SERS sensors also exhibited outstanding sensing performance for MB detection with limits of detectio...