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    • Ultrasensitive Detection of Methylene Blue Using an Electrochemically Synthesized SERS Sensor Based on Gold and Silver Nanoparticles: Roles of Composition and Purity on Sensing Performance and Reliability
    Tác giả : Mai Quan Doan; Nguyen Ha Anh; Nguyen Xuan Quang; Ngo Xuan Dinh; Doan Quang Tri; Tran Quang Huy; Anh-Tuan Le;  Người hướng dẫn: -;  Đồng tác giả: - (2021)

    An electrochemical approach has been used for green synthesis of gold and silver nanoparticles (e-AuNPs and e-AgNPs) with high levels of purity and scalability. The electrochemically synthesized noble-metal nanoparticles were characterized by ultraviolet–visible (UV–Vis) spectroscopy and scanning electron microscopy (SEM), confirming the formation of spherical e-AuNPs and e-AgNPs with average size of 19 nm and 24 nm, respectively. These green nanoparticles were deposited on aluminum substrates using the drop-drying method for surface-enhanced Raman scattering (SERS)-based detection of Methylene Blue (MB) within the ranges from 10−5 M to 10−8 M and 10−7 M to 10−10 M, respectively. The SERS sensors also exhibited outstanding sensing performance for MB detection with limits of detectio...
    • Novel Eco-Friendly Synthesis of Biosilver Nanoparticles as a Colorimetric Probe for Highly Selective Detection of Fe (III) Ions in Aqueous Solution
    Tác giả : Nguyen Le Nhat Trang; Van-Tuan Hoang; Ngo Xuan Dinh; Le Thi Tam; Van Phan Le; Dong Thi Linh; Doan Manh Cuong; Nguyen Tien Khi; Nguyen Ha Anh; Pham Tuyet Nhung; Anh-Tuan Le;  Người hướng dẫn: -;  Đồng tác giả: - (2021)

    In this work, an eco-friendly approach for the synthesis of biogenic silver nanoparticles (bio-AgNPs) using botanical extracts in combination with an electrochemical process was carried out. We employed three types of plant extracts, including green tea leaf (GTE), grapefruit peel (GP), and mangosteen peel (MP) extracts to successfully synthesize the bio-AgNPs and optimized the experimental conditions aiming to get the highest synthetic yield. The formation of bio-AgNPs was monitored by UV-Vis spectroscopy via a surface plasmon resonance (SPR) band at about 420–430 nm. Transmission electron microscope (TEM) showed their spherical shape with the size range within 23–55 nm. While X-ray diffraction (XRD) analysis described in detail the crystalline structure of the bio-AgNPs with a fac...